NMR spectroscopy : (Record no. 11184)

000 -LEADER
fixed length control field 06902nam a22003257a 4500
003 - CONTROL NUMBER IDENTIFIER
control field PK-SiUMT
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20220915111455.0
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
fixed length control field 220526b ||||| |||| 00| 0 eng d
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number 9783527330041 (hardcover)
020 ## - INTERNATIONAL STANDARD BOOK NUMBER
International Standard Book Number 9783527330003 (paperback)
040 ## - CATALOGING SOURCE
Transcribing agency PK-SiUMT
082 ## - DEWEY DECIMAL CLASSIFICATION NUMBER
Classification number 543.6
Item number GUN-N
100 1# - MAIN ENTRY--PERSONAL NAME
Personal name Günther, H.
Fuller form of name (Harald),
Relator term author.
9 (RLIN) 4452
240 10 - UNIFORM TITLE
Uniform title NMR Spektroskopie.
Language of a work English.
245 10 - TITLE STATEMENT
Title NMR spectroscopy :
Remainder of title basic principles, concepts, and applications in chemistry /
Statement of responsibility, etc. Harald Günther.
250 ## - EDITION STATEMENT
Edition statement Third, completely revised and updated edition.
264 #1 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Place of production, publication, distribution, manufacture Weinheim :
Name of producer, publisher, distributor, manufacturer Wiley-VCH,
Date of production, publication, distribution, manufacture, or copyright notice [2013?]
264 #4 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE
Date of production, publication, distribution, manufacture, or copyright notice ©2013
300 ## - PHYSICAL DESCRIPTION
Extent xvi, 718 pages :
Other physical details illustrations (some colour) ;
Dimensions 25 cm
500 ## - GENERAL NOTE
General note Translation of NMR-Spektroscopie: Grundlagen, Konzepte und Anwendungen der Protonen-und Kohlenstoff-13 Kernresonanz-Spektroscopie in der Chemie.
504 ## - BIBLIOGRAPHY, ETC. NOTE
Bibliography, etc. note Includes bibliographical references and index.
505 ## - FORMATTED CONTENTS NOTE
Formatted contents note TABLE OF CONTENTS
PREFACE

INTRODUCTION
Literature
Units and Constants

PART I: Basic Principles and Applications

THE PHYSICAL BASIS OF THE NUCLEAR MAGNETIC RESONANCE EXPERIMENT
The Quantum Mechanical Model for the Isolated Proton
Classical Description of the NMR Experiment
Experimental Verification of Quantized Angular Momentum and of the Resonance Equation
The NMR Experiment on Compact Matter and the Principle of the NMR Spectrometer
Magnetic Properties of Nuclei beyond the Proton

THE PROTON MAGNETIC RESONANCE SPECTRA OF ORGANIC MOLECULES - CHEMICAL SHIFT AND SPIN -
SPIN COUPLING
The Chemical Shift
Spin -
Spin Coupling

GENERAL EXPERIMENTAL ASPECTS OF NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
Sample Preparation and Sample Tubes
Internal and External Standards;
Solvent Effects
Tuning the Spectrometer
Increasing the Sensitivity
Measurement of Spectra at Different Temperatures

PROTON CHEMICAL SHIFTS AND SPIN -
SPIN COUPLING CONSTANTS AS FUNCTIONS OF STRUCTURE
Origin of Proton Chemical Shifts
Proton -
Proton Spin -
Spin Coupling and Chemical Structure

THE ANALYSIS OF HIGH-RESOLUTION NUCLEAR MAGNETIC RESONANCE SPECTRA
Notation for Spin Systems
Quantum Mechanical Formalism
The Hamilton Operator for High-Resolution Nuclear Magnetic Resonance Spectroscopy
Calculation of Individual Spin Systems

THE INFLUENCE OF MOLECULAR SYMMETRY AND CHIRALITY ON PROTON MAGNETIC RESONANCE SPECTRA
Spectral Types and Structural Isomerism
Influence of Chirality on the NMR Spectrum
Analysis of Degenerate Spin Systems by Means of 13C Satellites and H/D Substitution

PART II: Advanced Methods and Applications

THE PHYSICAL BASIS OF THE NUCLEAR MAGNETIC RESONANCE EXPERIMENT.
The NMR Signal by Pulse Excitation
Relaxation Effects
Pulse Fourier-Transform (FT) NMR Spectroscopy
Experimental Aspects of Pulse Fourier-Transform Spectroscopy
Double Resonance Experiments

TWO-DIMENSIONAL NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
Principles of Two-Dimensional NMR Spectroscopy
The Spin Echo Experiment in Modern NMR Spectroscopy
Homonuclear Two-Dimensional Spin Echo Spectroscopy: Separation of the Parameters J and d for Proton NMR Spectra
The COSY Experiment - Two-Dimensional 1H,1H Shift Correlations
The Product Operator Formalism
Phase Cycles
Gradient Enhanced Spectroscopy
Universal Building Blocks for Pulse Sequences
Homonuclear Shift Correlation by Double Quantum Selection of AX Systems - the 2D-INADEQUATE Experiment
Single-Scan 2D NMR

MORE 1D AND 2D NMR EXPERIMENTS: THE NUCLEAR OVERHAUSER EFFECT - POLARIZATION TRANSFER - SPIN LOCK EXPERIMENTS - 3D NMR
The Overhauser Effect
Polarization Transfer Experiments
Rotating Frame Experiments
Multidimensional NMR Experiments

CARBON-13 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
Historical Development and the Most Important Areas of Application
Experimental Aspects of Carbon-13 Nuclear Magnetic Resonance Spectroscopy
Carbon-13 Chemical Shifts
Carbon-13 Spin -
Spin Coupling Constants
Carbon-13 Spin -
Lattice Relaxation Rates

SELECTED HETERONUCLEI
Semimetals and Non-metals with the Exception of Hydrogen and Carbon
Main Group Metals
Transition Metals

INFLUENCE OF DYNAMIC EFFECTS ON NUCLEAR MAGNETIC RESONANCE SPECTRA
Exchange of Protons between Positions with Different Larmor Frequencies
Internal Dynamics of Organic Molecules
Intermolecular Exchange Processes
Line Broadening by Fast Relaxing Neighboring Nuclei

NUCLEAR MAGNETIC RESONANCE OF PARTIALLY ORIENTED MOLECULES AND SOLID STATE NMR
Nuclear Magnetic Resonance of Partially Oriented Molecules
High-Resolution Solid State Nuclear Magnetic Resonance Spectroscopy

SELECTED TOPICS OF NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
Isotope Effects in Nuclear Magnetic Resonance
Nuclear Magnetic Resonance Spectroscopy of Paramagnetic Materials
Chemically Induced Dynamic Nuclear Polarization (CIDNP)
Diffusion-Controlled Nuclear Magnetic Resonance Spectroscopy - DOSY
Unconventional Methods for Sensitivity Enhancement - Hyperpolarization
Nuclear Magnetic Resonance in Biochemistry and Medicine

INDEX
520 ## - SUMMARY, ETC.
Summary, etc. “Few good textbooks on NMR Spectroscopy are available at either the undergraduate or graduate levels. For those who want to go beyond elementary organic chemistry but without delving into all the mathematics Friebolin’s book is probably the best among this category.” (Journal of Chemical Education, 5 June 2014)

Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is
important for determining the 3D-structure of molecules.

This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Nuclear magnetic resonance spectroscopy.
9 (RLIN) 4453
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Spectroscopy
9 (RLIN) 4454
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Chemistry
9 (RLIN) 4455
650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element Biochemistry
9 (RLIN) 4456
856 ## - ELECTRONIC LOCATION AND ACCESS
Materials specified NMR spectroscopy Click here to access full text book
Uniform Resource Identifier https://pk1lib.org/book/2717626/ea87b0
942 ## - ADDED ENTRY ELEMENTS (KOHA)
Source of classification or shelving scheme
Koha item type Books
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Withdrawn status Lost status Source of classification or shelving scheme Damaged status Not for loan Permanent Location Current Location Shelving location Date acquired Source of acquisition Cost, normal purchase price Total Checkouts Full call number Barcode Date last seen Date last checked out Price effective from Koha item type
          Learning Resource Center University of Management and Technology, Sialkot City Campus Learning Resource Center University of Management and Technology, Sialkot City Campus General Stacks 05/26/2022 Star Books 12096.00 1 543.6 GUN-N 2013 12579 12579 07/10/2023 09/14/2022 05/26/2022 Books

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